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Bitumen production process

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1. Introduction
2. Bitumen production process
3. Benefits of air blowing method

1. Introduction

Bitumen is a main binder in road construction. It can be used to bond the aggregates well together and form the asphalt.
 
Different types of bitumen can be used in the flexible pavement. The main types of bitumen grades are VG bitumen and Pen bitumen which can be used directly in the hot asphalt.
 
These two types of bitumen are produced directly from distillation of crude oil. Generally, bitumen can be obtained by different ways including straight run, air blowing, semi blowing, solvent deasphalting and blending.
 
In the article below which is written by the Infinity Galaxy team, you can read more details about bitumen production by air blowing method. Also, the infographic can completely show you the bitumen production process.

2. Bitumen production process

Bitume production process infographics
Bitumen production is a complex process that involves several stages to convert crude oil into the final product suitable for various applications, particularly in road construction. Understanding the intricacies of this process is crucial for ensuring the quality and consistency of the end product.

2.1 Crude Oil Distillation

The journey of bitumen production begins with the refining of crude oil in a petroleum refinery. Crude oil, extracted from geological formations, is a mixture of hydrocarbons of varying molecular weights and compositions. In the first stage of the process, known as crude oil distillation, the crude oil is heated in a distillation unit, typically consisting of an atmospheric distillation tower.

As the crude oil is heated, it vaporizes and rises through the tower, which contains multiple trays or stages. Each tray allows for the separation of different components of the crude oil based on their boiling points and molecular weights. Lighter components, such as gasoline and diesel, vaporize at lower temperatures and are collected from higher trays, while heavier components, including bitumen precursors, remain in liquid form and are collected at the bottom of the tower.

2.2 Vacuum Distillation

After the initial distillation process, the heavier residue known as "long residue" or "residuum" is further processed in a vacuum distillation tower. This residual fraction contains high molecular weight hydrocarbons, including the precursors for bitumen production. Vacuum distillation is conducted under reduced pressure to lower the boiling point of the residual fraction, preventing thermal degradation and reducing the risk of unwanted reactions.

During vacuum distillation, the long residue is heated and vaporized, allowing for the separation of additional fractions based on their boiling points. The heaviest fraction obtained from vacuum distillation is known as "vacuum bottom," which serves as a primary feedstock for bitumen production.

2.3 Air Blowing and Oxidation

The vacuum bottom obtained from the vacuum distillation tower undergoes further processing through air blowing and oxidation to convert it into bitumen. In the air blowing process, the vacuum bottom is heated and exposed to controlled airflow, typically using mild air or oxygen. This introduction of air leads to the oxidation of bitumen precursors, resulting in changes to its chemical composition and physical properties.

The oxidation process influences critical characteristics of the final bitumen product, such as its softening point, penetration degree, and viscosity. Through careful control of process parameters, different grades of bitumen can be produced to meet specific performance requirements for various applications, including road construction.

2.4 Product Refinement and Packaging

Following the air blowing and oxidation steps, the resulting bitumen undergoes quality control measures to ensure that it meets industry standards and specifications. Quality testing may include analyses of viscosity, penetration, ductility, and other physical properties, as well as assessments of chemical composition and performance characteristics.

Once the quality of the bitumen is confirmed, it is packaged into containers suitable for distribution and storage. Common packaging options include new steel drums or jumbo bags, which protect the bitumen from contamination and ensure its integrity during transportation to end-users, such as construction companies and infrastructure developers.

3. Benefits of Air Blowing Method

The air blowing method, also known as the oxidation process, plays a pivotal role in the production of bitumen from vacuum bottom obtained during crude oil refining. This method offers several distinct advantages over alternative processes, making it a preferred choice for bitumen manufacturers. Understanding the benefits of the air blowing method is essential for optimizing bitumen production processes and enhancing product quality.

3.1 Enhanced Control over Bitumen Properties

One of the primary advantages of the air blowing method is its ability to provide precise control over the properties of the resulting bitumen. By adjusting key parameters such as temperature, airflow rate, and reaction time, manufacturers can tailor the characteristics of the bitumen to meet specific performance requirements. This level of control allows for the production of bitumen grades with varying viscosity, penetration, softening point, and other critical attributes, ensuring compatibility with diverse applications in road construction and other industries.

3.2 Modification of Physical and Chemical Properties

The oxidation process facilitated by air blowing induces significant changes in the molecular structure of bitumen precursors present in the vacuum bottom feedstock. Through controlled exposure to air or oxygen, chemical reactions occur, leading to the formation of oxygen-containing functional groups within the bitumen matrix. These structural modifications impart desirable properties to the bitumen, such as improved elasticity, adhesion, and resistance to aging and weathering. Additionally, oxidation facilitates the enhancement of thermal stability and rheological properties, further enhancing the performance and durability of the final bitumen product.

3.3 Versatility in Bitumen Grade Production

Another key benefit of the air blowing method is its versatility in producing a wide range of bitumen grades to suit varying application requirements. By manipulating process parameters and reaction conditions, manufacturers can generate different viscosity grades, penetration grades, and performance grades of bitumen. This flexibility allows for the customization of bitumen products tailored to specific climate conditions, traffic loads, and pavement specifications. Furthermore, the air blowing method enables the production of specialized bitumen variants, such as modified bitumen and polymer-modified bitumen, which exhibit enhanced properties for specialized applications in high-traffic areas, extreme weather environments, and challenging construction scenarios.

3.4 Environmental and Economic Considerations

In addition to its technical advantages, the air blowing method offers environmental and economic benefits compared to alternative bitumen production processes. The oxidation process consumes relatively less energy and generates fewer greenhouse gas emissions compared to alternative methods such as solvent extraction or thermal cracking. Furthermore, the utilization of vacuum bottom, a by-product of crude oil refining, as the primary feedstock for bitumen production enhances resource efficiency and reduces waste disposal requirements. Overall, the air blowing method contributes to sustainable manufacturing practices while maintaining cost competitiveness in the bitumen industry.

4. Quality Control and Testing Procedures

Ensuring the quality and consistency of bitumen products is paramount in meeting the stringent performance requirements of infrastructure projects, particularly in road construction. Quality control measures and rigorous testing procedures are integral components of the bitumen production process, allowing manufacturers to assess and verify the physical, chemical, and performance characteristics of the final product. This section provides an overview of the key quality control and testing procedures employed in bitumen production facilities.

4.1 Physical Properties Testing

Physical properties testing encompasses a range of analyses aimed at evaluating the fundamental characteristics of bitumen related to its mechanical behavior, durability, and suitability for specific applications. Common physical properties tests conducted on bitumen samples include:

Penetration Test: This test measures the consistency of bitumen by determining the depth to which a standard needle penetrates the material under specified conditions. Penetration values indicate the hardness or softness of bitumen and are used to classify bitumen into penetration grade categories.

Softening Point Test: The softening point of bitumen is determined using methods such as the ring and ball apparatus, indicating the temperature at which the bitumen softens and flows under standardized conditions. This parameter is crucial for assessing the temperature susceptibility and thermal stability of bitumen in pavement applications.

Ductility Test: Ductility represents the ability of bitumen to stretch without breaking and is evaluated by measuring the elongation of a bitumen sample before failure under tension. Ductility values provide insights into the flexibility and deformation resistance of bitumen at different temperatures and loading conditions.

Viscosity Test: Viscosity is a measure of bitumen's resistance to flow and deformation, affecting its handling characteristics and coating ability. Various viscosity testing methods, including rotational viscometry and capillary viscometry, are employed to quantify bitumen viscosity at specific temperatures and shear rates.

4.2 Chemical Composition Analysis

Chemical composition analysis plays a crucial role in assessing the purity, stability, and performance-enhancing additives present in bitumen formulations. Advanced analytical techniques are utilized to characterize the molecular structure and functional groups within bitumen samples, including:

Gas Chromatography-Mass Spectrometry (GC-MS): GC-MS analysis allows for the identification and quantification of individual hydrocarbon components present in bitumen, facilitating the determination of molecular weight distribution, aromaticity, and heterogeneity.

Fourier Transform Infrared Spectroscopy (FTIR): FTIR spectroscopy provides insights into the chemical bonding and functional groups present in bitumen molecules, enabling the detection of oxidation products, polymer additives, and other chemical modifiers.

4.3 Performance Testing

Performance testing evaluates the functional properties of bitumen related to its behavior under simulated service conditions, such as traffic loading, temperature variations, and moisture exposure. Performance tests assess key parameters, including:

Rheological Properties: Dynamic Shear Rheometer (DSR) and Bending Beam Rheometer (BBR) tests measure the viscoelastic behavior and stiffness characteristics of bitumen at different temperatures and loading frequencies, reflecting its deformation resistance and fatigue performance.

Aging Resistance: Thin Film Oven Test (TFOT) and Pressure Aging Vessel (PAV) tests simulate the effects of short-term and long-term aging on bitumen samples, assessing their resistance to oxidative aging, hardening, and embrittlement over time.

4.4 Quality Assurance Protocols

In addition to laboratory testing, quality assurance protocols are implemented throughout the bitumen production process to ensure compliance with industry standards and specifications. Quality assurance measures include:

Process Control Monitoring: Continuous monitoring of process parameters, such as temperature, pressure, and flow rates, ensures the consistent production of bitumen with predetermined properties and characteristics.

Batch Sampling and Analysis: Regular sampling of bitumen batches at various stages of production allows for real-time quality assessment and adjustment of process parameters to maintain product consistency and integrity.

Certification and Compliance: Bitumen products undergo third-party certification and compliance testing to validate their conformity with national and international standards, ensuring their suitability for use in construction projects and infrastructure applications.